6-chloro-1-methyl-2-indolinethione

Base Information

Chemical Name:6-chloro-1-methyl-2-indolinethione
CAS No.:156136-70-8
Molecular Formula:C₉H₈ClNS
Molecular Weight:197.688
Hs Code.:

Synonyms:6-chloro-1-methyl-2-indolinethione

Suppliers and Price of 6-chloro-1-methyl-2-indolinethione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 6-chloro-1-methyl-2-indolinethione

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-chloro-1-methyl-2-indolinethione

There total 1 articles about 6-chloro-1-methyl-2-indolinethione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6341-92-0
6-chloroisatin

: 156136-70-8
6-chloro-1-methyl-2-indolinethione

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / ethanol / 0.5 h / Heating

2: Na / ethanol / Heating

3: NaOH / H₂O / Heating

4: 87 percent / Na₂CO₃, P₂S₅ / tetrahydrofuran / Ambient temperature

With sodium hydroxide; tetraphosphorus decasulfide; sodium; sodium carbonate; hydrazine hydrate; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jm00039a016

Reference yield: 98.0%

: 175789-33-0
3-styryl-1,2-benzoisothiazole-1,1-dioxide

: 156136-70-8
6-chloro-1-methyl-2-indolinethione

: (3S,4'R)-7'-chloro-9'-methyl-4'-phenyl-4',9'-dihydro-2H,3'H-spiro[benzo[d]isothiazole-3,2'-thiopyrano[2,3-b]indole] 1,1-dioxide

Guidance literature:: With 1-(3,5-bis(trifluoromethyl)phenyl)-3-((S)-(6-methoxyquinolin-4-yl)((2S,4S,8R)-8-vinylquinuclidin-2-yl)methyl)thiourea; In toluene; at -10 ℃; for 40h; enantioselective reaction; Molecular sieve;
DOI:10.1021/acs.orglett.5b01951

Reference yield: 96.0%

: 2700-22-3
Benzylidenemalononitrile

: 156136-70-8
6-chloro-1-methyl-2-indolinethione

: C₁₉H₁₄ClN₃S

Guidance literature:: Benzylidenemalononitrile; With C₂₆H₂₄F₆N₂S; In 1,3,5-trimethyl-benzene; at -10 ℃; for 0.5h; Molecular sieve;

6-chloro-1-methyl-2-indolinethione; In 1,3,5-trimethyl-benzene; for 30h;