rac-1-Chlor-2-methyl-3-phenylpropan

Base Information

• Chemical Name: rac-1-Chlor-2-methyl-3-phenylpropan
• CAS No.: 73756-58-8
• Molecular Formula: C₁₀H₁₃Cl
• Molecular Weight: 168.666
• Mol file: 73756-58-8.mol

Synonyms:rac-1-Chlor-2-methyl-3-phenylpropan

Chemical Property of rac-1-Chlor-2-methyl-3-phenylpropan

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of rac-1-Chlor-2-methyl-3-phenylpropan

There total 6 articles about rac-1-Chlor-2-methyl-3-phenylpropan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.5%

→ rac-1-Chlor-2-methyl-3-phenylpropan (73756-58-8) + 2-methyl-3-(p-tert-butylphenyl)-propyl chloride (73756-69-1)

Guidance literature:

Reference yield: 74.3%

2-methyl-3-phenylpropanol (22436-06-2,77943-96-5,78964-61-1,7384-80-7) → rac-1-Chlor-2-methyl-3-phenylpropan (73756-58-8)

Guidance literature:

With thionyl chloride; In chloroform; at 140 ℃; for 3h;

Reference yield:

→ ((R)-γ-chloro-isobutyl)-benzene (24435-51-6,73756-58-8)

Guidance literature:

With pyridine; thionyl chloride;

DOI:10.1021/ja01589a039

upstream raw materials:

2-methyl-3-phenylpropanol

(Z)-α-methyl-cinnamaldehyde

2-methyl-3-phenylpropanoic acid

2-benzyl-2-methylmalonic acid

Downstream raw materials:

(2-methyl-3-phenyl-propyl)-malonic acid diethyl ester

3-[4-(1,1-dimethylpentyl)-phenyl]-2-methylpropyl chloride

(2-methyl-3-phenyl-propyl)-malonic acid

4-methyl-5-phenylpentanoic acid

Refernces

• 1、 -. "Substituted phenylpropyl halides". . . Retrieved 2008/06/13.