ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate

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Chemical Name:ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate
CAS No.:1400898-77-2
Molecular Formula:C₂₀H₁₇ClN₂O₂S
Molecular Weight:384.886
Hs Code.:

Synonyms:ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate

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Technology Process of ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate

There total 2 articles about ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 136-95-8,102337-98-4,84293-42-5
2-amino-benzthiazole

: 141-97-9
ethyl acetoacetate

: 587-04-2
m-Chlorobenzaldehyde

: 1400898-77-2
ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate

Guidance literature:: With poly(ethylene glycol); at 20 ℃; for 1.2h; Green chemistry;
DOI:10.2174/1570178612666150113231342

Reference yield:

: 873-63-2
m-chlorobenzyl alcohol

: 1400898-77-2
ethyl 4-(3-chlorophenyl)-2-methyl-4H-benzo[4,5]thiazolo[3,2-a]pyrimidine-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Rose Bengal lactone; oxygen / water / 24 h / 30 °C / Irradiation; Green chemistry

2: trypsin / water / 48 h / 50 °C / Green chemistry; Enzymatic reaction

With oxygen; Rose Bengal lactone; trypsin; In water; 2: |Biginelli Pyrimidone Synthesis;
DOI:10.1016/j.bioorg.2020.104534