4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

Base Information

Chemical Name:4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine
CAS No.:217318-36-0
Molecular Formula:C₂₂H₂₁NO₃
Molecular Weight:347.414
Hs Code.:

Synonyms:4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

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Technology Process of 4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

There total 12 articles about 4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1423-60-5
methyl ethynyl ketone

: 217318-33-7
1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

: 217318-36-0
4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

Guidance literature:: methyl ethynyl ketone; 1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine; In toluene; for 20h;

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; for 12h;

Reference yield:

: 1423-60-5
methyl ethynyl ketone

: 84-58-2
2,3-dicyano-5,6-dichloro-p-benzoquinone

: 217319-31-8
1-Ethyl-7-methoxy-2-(4-methoxyphenyl)-indolizine

: 217318-36-0
4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

Guidance literature:: In toluene;

Reference yield:

: 217303-03-2
4-methoxy-2-n-propylpyridine-N-oxide

: 217318-36-0
4-acetyl-1-ethyl-6-methoxy-2-(4-methoxyphenyl)pyrrolo[2,1,5-cd]indolizine

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid; zinc / water / 12 h / 70 - 80 °C

2.1: acetone / 8 h / Heating / reflux

3.1: sodium hydrogencarbonate / water / 2 h / Heating / reflux

4.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 1 h / Heating / reflux

5.1: potassium hydroxide / methanol / 10 h / Heating / reflux

6.1: hydrogenchloride; water

7.1: copper / quinoline / 8 h / 170 °C

8.1: toluene / 20 h

8.2: 12 h

With hydrogenchloride; potassium hydroxide; sulfuric acid; water; sodium hydrogencarbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; zinc; copper; In quinoline; methanol; water; acetone; toluene;