4-methylphenyl 2-allyl disulfide

Base Information

• Chemical Name: 4-methylphenyl 2-allyl disulfide
• CAS No.: 81650-47-7
• Molecular Formula: C₁₀H₁₂S₂
• Molecular Weight: 196.337

Synonyms:4-methylphenyl 2-allyl disulfide

Chemical Property of 4-methylphenyl 2-allyl disulfide

Chemical Property:

Purity/Quality:

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Technology Process of 4-methylphenyl 2-allyl disulfide

There total 4 articles about 4-methylphenyl 2-allyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

para-thiocresol (106-45-6) + SS-prop-2-enyl-2-methyldithioperoxypropanoate (118087-48-2) → 4-methylphenyl 2-allyl disulfide (81650-47-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In pentane; for 2h; Ambient temperature;

DOI:10.1055/s-1994-25563

Reference yield:

1-p-tolylsulfanyl-1H-benzotriazole; hydrochloride + prop-2-ene-1-thiol (870-23-5) → diallyl disulphide (2179-57-9) + di(p-tolyl) disulfide (103-19-5) + 4-methylphenyl 2-allyl disulfide (81650-47-7)

Guidance literature:

In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1021/jo060693n

Reference yield:

1-p-tolylsulfanyl-1H-benzotriazole + prop-2-ene-1-thiol (870-23-5) → 4-methylphenyl 2-allyl disulfide (81650-47-7)

Guidance literature:

In dichloromethane; at -20 - 0 ℃; for 0.5h;

DOI:10.1016/j.bioorg.2021.104814

upstream raw materials:

para-thiocresol

SS-prop-2-enyl-2-methyldithioperoxypropanoate

prop-2-ene-1-thiol

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