2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

Base Information

Chemical Name:2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone
CAS No.:1422964-62-2
Molecular Formula:C₂₄H₂₉IO₇S
Molecular Weight:588.461
Hs Code.:

Synonyms:2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

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Chemical Property of 2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

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Technology Process of 2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

There total 3 articles about 2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1422964-63-3
C₂₅H₃₂O₁₀S₂

: 1422964-62-2
2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1021/jo3024973

Reference yield:

: 1430222-66-4
C₂₃H₂₈O₆

: 1422964-62-2
2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane

2: potassium iodide / N,N-dimethyl-formamide / 50 °C

With pyridine; potassium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo3024973

Reference yield:

: 776313-91-8
3-[2',3'-di-O-benzyl-α-D-glucopyranosyl]-1-propene

: 1422964-62-2
2-C-(6-iodo-2,3-di-O-benzyl-4-O-mesyl-6-deoxy-α-D-glucopyranosyl)acetone

Guidance literature:: Multi-step reaction with 3 steps

1: palladium dichloride; copper dichloride / N,N-dimethyl-formamide; water

2: pyridine / dichloromethane

3: potassium iodide / N,N-dimethyl-formamide / 50 °C

With pyridine; potassium iodide; copper dichloride; palladium dichloride; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo3024973