2,3-dimethoxybenzamide oxime

Base Information

• Chemical Name: 2,3-dimethoxybenzamide oxime
• CAS No.: 407610-22-4
• Molecular Formula: C₉H₁₂N₂O₃
• Molecular Weight: 196.206
• Mol file: 407610-22-4.mol

Synonyms:2,3-dimethoxybenzamide oxime

Chemical Property of 2,3-dimethoxybenzamide oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-dimethoxybenzamide oxime

There total 2 articles about 2,3-dimethoxybenzamide oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2,3-dimethoxybenzonitrile (5653-62-3) → 2,3-dimethoxybenzamide oxime (407610-22-4,1654022-08-8)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; for 16h; Heating;

DOI:10.1016/S0968-0896(01)00175-4

Reference yield:

→ N-hydroxy-2,3-dimethoxy-benzamidine (407610-22-4)

Guidance literature:

Reference yield: 66.0%

1-benzylpiperidine-2-carboxylic acid methyl ester (124619-69-8) + 2,3-dimethoxybenzamide oxime (407610-22-4,1654022-08-8) → 1-benzyl-2-[3-(2,3-dimethoxy-phenyl)-[1,2,4]oxadiazol-5-yl]-piperidine

Guidance literature:

2,3-dimethoxybenzamide oxime; With sodium hydride; In tetrahydrofuran; Heating;

1-benzylpiperidine-2-carboxylic acid methyl ester; In tetrahydrofuran; Heating;

DOI:10.1016/S0968-0896(01)00175-4

upstream raw materials:

2,3-dimethoxybenzonitrile