Technology Process of 2-bromo-4-fluorobenzaldehyde oxime
There total 1 articles about 2-bromo-4-fluorobenzaldehyde oxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium hydrogencarbonate;
In
ethanol; water;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/acs.orglett.7b03776
- Guidance literature:
-
With
ammonium thiocyanate; fluorescein sodium salt;
In
acetonitrile;
at 20 ℃;
for 10h;
Irradiation;
DOI:10.1039/c9cc05354a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: zinc; hydrogenchloride / ethanol; water / 2 h / 0 - 20 °C / Inert atmosphere
2: triethylamine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
3: palladium diacetate; 1,1'-bis(di-tertbutylphosphino)ferrocene; cesium fluoride; tributyltin fluoride / toluene / 2 h / 100 °C
With
hydrogenchloride; 1,1'-bis(di-tertbutylphosphino)ferrocene; palladium diacetate; tributyltin fluoride; triethylamine; cesium fluoride; zinc;
In
ethanol; dichloromethane; water; toluene;
DOI:10.1021/acs.orglett.7b03776
