(Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

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Chemical Name:(Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate
CAS No.:1450880-87-1
Molecular Formula:C₄₇H₅₂N₂O₄Si₂
Molecular Weight:765.112
Hs Code.:

Synonyms:(Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

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Chemical Property of (Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

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Technology Process of (Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

There total 4 articles about (Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 73043-35-3
(Z)-4-(4-(4-hydroxybenzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazole-1-yl)butanoic acid

: 1450880-87-1
(Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

Guidance literature:: With 1H-imidazole; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 30h;
DOI:10.1039/c3ob41341a

Reference yield:

: 52507-17-2,60470-81-7
(Z)-4-((2-methyl-5-oxooxazol-4(5H)-ylidene)methyl)phenyl acetate

: 1450880-87-1
(Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine; water / ethanol / 3 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / Reflux

2.2: pH Ca_. 5 / Acidic conditions

3.1: 1H-imidazole; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 30 h

With 1H-imidazole; water; caesium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41341a

Reference yield:

: C₁₇H₁₈N₂O₅

: 1450880-87-1
(Z)-tert-butyldiphenylsilyl 4-(4-(4-((tert-butyldiphenylsilyl)-oxy)benzylidene)-2-methyl-5-oxo-4,5-dihydro-1H-imidazol-1-yl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.25 h / Reflux

1.2: pH Ca_. 5 / Acidic conditions

2.1: 1H-imidazole; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 30 h

With 1H-imidazole; caesium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c3ob41341a