3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol

Base Information

Chemical Name:3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol
CAS No.:131573-02-9
Molecular Formula:C₂₅H₂₇NO₄S
Molecular Weight:437.56
Hs Code.:

Synonyms:3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol

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Technology Process of 3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol

There total 2 articles about 3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 131572-99-1
O,O-bis(trimethylsilyl)-3-methyl-4,5-dihydrocatechol

: 124337-85-5
α,α-dimethyl-1-(p-toluenesulfonyl)-1H-indole-4-methanol

: 131573-03-0
4-Isopropenyl-1-(toluene-4-sulfonyl)-1H-indole

: 131573-02-9
3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol

Guidance literature:: With tin(IV) chloride; In dichloromethane; at -75 ℃; for 0.25h;
DOI:10.1016/S0040-4020(01)96005-3

Reference yield:

: 31271-85-9
4-methoxycarbonyl-1-<(4-methylphenyl)sulfonyl>-1H-indole

: 131573-02-9
3-methyl-6-<1-methyl-1-(1-p-toluenesulfonyl-4-indolyl)ethyl>-1,2-cyclohexanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / diethyl ether; tetrahydrofuran / 1) 0 deg C, 10 min, 2) RT, 20 min

2: 69 percent / SnCl₄ / CH₂Cl₂ / 0.25 h / -75 °C

With tin(IV) chloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)96005-3