2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

Base Information

Chemical Name:2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine
CAS No.:177172-32-6
Molecular Formula:C₂₂H₂₀ClN₃O
Molecular Weight:377.873
Hs Code.:

Synonyms:2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

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Chemical Property of 2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

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Technology Process of 2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

There total 5 articles about 2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 95-54-5
1,2-diamino-benzene

: 177172-24-6
(E)-1-(2-Chloro-6-ethoxy-pyridin-4-yl)-3-phenyl-propenone

: 177172-32-6
2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

Guidance literature:: In butan-1-ol; for 12h; Heating;

Reference yield:

: 1604-14-4
2,6-dichloroisonicotinic acid ethyl ester

: 177172-32-6
2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / Na / 16 h / 80 - 90 °C

2: 45 percent / 25percent aq. H₂SO₄ / 12 h / Heating

3: 70 percent / Et₃N, Et₂NH / ethanol / Heating

4: 60 percent / butan-1-ol / 12 h / Heating

With sulfuric acid; sodium; diethylamine; triethylamine; In ethanol; butan-1-ol;

Reference yield:

: 100-52-7
benzaldehyde

: 177172-32-6
2-(2-Chloro-6-ethoxy-pyridin-4-yl)-4-phenyl-2,3-dihydro-1H-benzo[b][1,4]diazepine

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Et₃N, Et₂NH / ethanol / Heating

2: 60 percent / butan-1-ol / 12 h / Heating

With diethylamine; triethylamine; In ethanol; butan-1-ol;