3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French]

Base Information

Chemical Name:3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French]
CAS No.:83868-31-9
Molecular Formula:C₆H₃N₃O₇*C₁₄H₁₈N₂O
Molecular Weight:459.415
Hs Code.:
DSSTox Substance ID:DTXSID20232765

Synonyms:3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French];83868-31-9;3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate;DTXSID20232765;C14H18N2O.C6H3N3O7;LS-127368;C14-H18-N2-O.C6-H3-N3-O7

Suppliers and Price of 3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French]

Chemical Property:

Vapor Pressure:2.78E-06mmHg at 25°C
Boiling Point:389.8°C at 760 mmHg
Flash Point:189.5°C
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:2
Exact Mass:459.13901265
Heavy Atom Count:33
Complexity:561

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)CC1=CNC2=C1C=CC3=C2CCCO3.C1=C(C=C(C(=C1[N+](=O)[O-])O)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French]

There total 6 articles about 3-(7,8,9-Trihydro-pyranno(2,3-g)indolyl)-N,N-dimethylmethylamine picrate [French] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 88-89-1
2,4,6-Trinitrophenol

: 81258-00-6
tetrahydro-1,7,8,9 pyranno<2,3-g>indolyl-3 N,N-dimethylamine

: 83868-31-9
Dimethyl-(1,7,8,9-tetrahydro-pyrano[2,3-g]indol-3-ylmethyl)-amine; compound with picric acid

Guidance literature:: In ethanol; for 12h; Ambient temperature;
DOI:10.1139/v82-298

Reference yield:

: 55745-97-6
3,4-dihydro-2H-1-benzopyran-6-carbaldehyde

: 83868-31-9
Dimethyl-(1,7,8,9-tetrahydro-pyrano[2,3-g]indol-3-ylmethyl)-amine; compound with picric acid

Guidance literature:: Multi-step reaction with 6 steps

1: Na / methanol / 6 h / 0 °C

2: 42 percent / N₂ / xylene / 5 h / Heating

3: 83 percent / 1) KOH, H₂O; 2) 5 N HCl / 1) reflux, 3.5 h; 2) 0 deg C

4: 83 percent / CuO, Cr₂O₃ / quinoline / 7.5 h / 190 - 195 °C

5: 58 percent / methanol / 72 h / Heating

6: 93 percent / ethanol / 12 h / Ambient temperature

With hydrogenchloride; chromium(III) oxide; potassium hydroxide; nitrogen; water; sodium; copper(II) oxide; In quinoline; methanol; ethanol; xylene;
DOI:10.1139/v82-298

Reference yield:

: 81257-90-1
acide tetrahydro-1,7,8,9-pyranno<2,3-g>indolecarboxylique-2

: 83868-31-9
Dimethyl-(1,7,8,9-tetrahydro-pyrano[2,3-g]indol-3-ylmethyl)-amine; compound with picric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / CuO, Cr₂O₃ / quinoline / 7.5 h / 190 - 195 °C

2: 58 percent / methanol / 72 h / Heating

3: 93 percent / ethanol / 12 h / Ambient temperature

With chromium(III) oxide; copper(II) oxide; In quinoline; methanol; ethanol;
DOI:10.1139/v82-298