allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate

Base Information

• Chemical Name: allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate
• CAS No.: 1022160-23-1
• Molecular Formula: C₅₈H₆₈N₆O₁₂
• Molecular Weight: 1041.21

Synonyms:allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate

Chemical Property of allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate

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Technology Process of allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate

There total 1 articles about allyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

allyl L-3-(N-acetyl-N-benzyloxy)aminoalaninate (1022160-21-9) + N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycine (1022160-17-3) → allyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate (1022160-23-1)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 94.0%

allyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalaninate (1022160-23-1) → N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalanine (1022160-18-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1016/j.tetlet.2008.02.007

upstream raw materials:

allyl L-3-(N-acetyl-N-benzyloxy)aminoalaninate

N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

Downstream raw materials:

N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinyl-L-3-(N-acetyl-N-benzyloxy)aminoalanine

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