6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

Base Information

Chemical Name:6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene
CAS No.:1026701-97-2
Molecular Formula:C₁₈H₂₆O₃Si
Molecular Weight:318.488
Hs Code.:

Synonyms:6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

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Chemical Property of 6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

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Technology Process of 6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

There total 1 articles about 6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112043-57-9
2-(3-iodopropyl)furan

: 71504-29-5
methyl o-(trimethylsilyl)benzoate

: 1026701-97-2
6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

Guidance literature:: With penta-1,3-diene; ammonia; lithium; In tetrahydrofuran; tert-butyl alcohol; at -78 ℃; for 1h;
DOI:10.1021/jo000209v

Reference yield:

: 1026701-97-2
6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

: [1-(3-furan-2-yl-propyl)-2-trimethylsilanyl-cyclohexa-2,5-dienyl]-methanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1021/jo000209v

Reference yield:

: 1026701-97-2
6-carbomethoxy-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

: 1026982-20-6
6-acetoxymethyl-6-(3'-(2'-furanyl)propyl)-1-(trimethylsilyl)-1,4-cyclohexadiene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 0.5 h / 0 °C

2: pyridine; DMAP / 20 °C

With pyridine; dmap; lithium aluminium tetrahydride; In diethyl ether; 1: Reduction / 2: Acylation;
DOI:10.1021/jo000209v