N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

Base Information

Chemical Name:N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine
CAS No.:130945-21-0
Molecular Formula:C₅₅H₈₂N₂O₁₀S₄
Molecular Weight:1059.53
Hs Code.:

Synonyms:N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

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Chemical Property of N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

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Technology Process of N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

There total 8 articles about N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 130945-17-4
N,N'-bis(9-hydroxynonyl)-N,N'-di-p-toluenesulfonyl-1,9-nonanediamine

: 104-15-4
toluene-4-sulfonic acid

: 130945-21-0
N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

Guidance literature:: With N,N'-dimethylaminopyridine; triethylamine; In dichloromethane; for 2.5h; Ambient temperature;

Reference yield:

: 55362-80-6
9-bromononan-1-ol

: 130945-21-0
N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / p-toluenesulfonic acid / diethyl ether / 14 h / Ambient temperature

2: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg 2.) DMF, 60 deg C, 3 h

3: 100 percent / p-toluenesulfonyl chloride / methanol / 0.33 h / Ambient temperature

4: 95 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

With N,N'-dimethylaminopyridine; sodium hydride; toluene-4-sulfonic acid; triethylamine; p-toluenesulfonyl chloride; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 55695-90-4
2-(9-bromononyloxy)tetrahydropyran

: 130945-21-0
N,N'-di-p-toluenesulfonyl-N,N'-bis<9-(p-toluenesulfonyloxy)nonyl>-1,9-nonanediamine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMF, 60 deg C, 20 to 25 mm Hg 2.) DMF, 60 deg C, 3 h

2: 100 percent / p-toluenesulfonyl chloride / methanol / 0.33 h / Ambient temperature

3: 95 percent / triethylamine, N,N'-dimethylaminopyridine / CH₂Cl₂ / 2.5 h / Ambient temperature

With N,N'-dimethylaminopyridine; sodium hydride; triethylamine; p-toluenesulfonyl chloride; In methanol; dichloromethane;