p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:916497-83-1
Molecular Formula:C₃₈H₄₉NO₉S
Molecular Weight:695.874
Hs Code.:

Synonyms:p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 10022-13-6,31505-44-9,81704-02-1,116347-84-3,131234-07-6,144300-04-9,79733-86-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranose

: 20025-90-5
p-dodecylbenzenethiol

: 916497-83-1
p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2006.08.095

Reference yield: 92.0%

: 916497-83-1
p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1010692-61-1
(2R,4aR,6S,7S,8R,8aR)-8-Benzyloxy-2-phenyl-6-[(2R,3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-2-ylmethoxy]-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1010692-62-2
C₇₂H₈₁NO₂₀Si

Guidance literature:: With N-iodo-succinimide; silver trifluoromethanesulfonate; In dichloromethane; at -50 ℃;
DOI:10.1016/j.bmcl.2006.08.095

Reference yield:

: 916497-83-1
p-dodecylphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1010692-64-4
N-(2-{8-benzyloxy-2-phenyl-6-[3,4,5-tris-benzyloxy-6-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-2-ylmethoxy]-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxy}-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / N-iodosuccinimide; silver triflate / CH₂Cl₂ / -50 °C

2: hydrazine hydrate

3: pyridine

4: sodium methoxide

With pyridine; N-iodo-succinimide; sodium methylate; silver trifluoromethanesulfonate; hydrazine hydrate; In dichloromethane;
DOI:10.1016/j.bmcl.2006.08.095