4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

Base Information

Chemical Name:4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide
CAS No.:1159276-65-9
Molecular Formula:C₁₉H₁₂F₁₇NO
Molecular Weight:593.283
Hs Code.:

Synonyms:4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

Suppliers and Price of 4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

There total 1 articles about 4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1159276-64-8
N-{4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl}-formamide

: 1159276-65-9
4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

Guidance literature:: With bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; for 1h; Inert atmosphere;
DOI:10.1002/ejic.200701341

Reference yield: 91.0%

: 1159276-65-9
4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

: silver nitrate

: [Ag(4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-hepradecafluorododecyl)oxo]phenylisocyanide)2][NO₃]

Guidance literature:: In tetrahydrofuran; N2; ligand (0.62 mmol) soln. in THF added dropwise to THF soln. of Ag compd. (0.29 mmol) with stirring, stirred in dark for 4 h; pptd. (Et2O), filtered off, dried (P2O5, vac., 16 h), elem. anal.;
DOI:10.1002/ejic.200701341

Reference yield: 84.0%

: 1159276-65-9
4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-heptadecafluorododecyl)oxy]phenyl isocyanide

: copper(l) chloride

: 1159276-58-0
[CuCl(4-[(5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,12-hepradecafluorododecyl)oxo]phenylisocyanide)]

Guidance literature:: In tetrahydrofuran; N2; ligand (0.549 mmol) soln. in THF added dropwise to THF soln. of Cu compd. (0.51 mmol) with stirring, stirred for 1.5 h; pptd. (hexane), filtered off, dried (vac.), elem. anal.;
DOI:10.1002/ejic.200701341