2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

Base Information

Chemical Name:2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride
CAS No.:1353758-40-3
Molecular Formula:C₁₆H₂₁NO₄S*ClH
Molecular Weight:359.874
Hs Code.:

Synonyms:2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

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Chemical Property of 2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

Chemical Property:

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Technology Process of 2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

There total 5 articles about 2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1353758-87-8
methyl 2-((4-(2-methyl-2-morpholinopropanoyl)phenyl)thio)acetate

: 1353758-40-3
2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

Guidance literature:: With hydrogenchloride; In water; at 25 ℃;

Reference yield:

: 903635-99-4
2-(4-bromophenyl)-2-methoxy-3,3-dimethyl-oxirane

: 1353758-40-3
2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 21 h / 130 °C

2: N-ethyl-N,N-diisopropylamine / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 21 h / Reflux

3: hydrogenchloride / water / 25 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; water;

Reference yield:

: 49660-93-7
4'-bromoisobutyrophenone

: 1353758-40-3
2-[4-(2-methyl-2-morpholin-4-ium-4-yl-propanoyl)phenyl]sulfanylacetic acid chloride

Guidance literature:: Multi-step reaction with 5 steps

1: bromine; chlorosulfonic acid / chlorobenzene / 20 °C

2: chlorobenzene; methanol / 1.5 h / 20 °C

3: 21 h / 130 °C

4: N-ethyl-N,N-diisopropylamine / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 21 h / Reflux

5: hydrogenchloride / water / 25 °C

With hydrogenchloride; chlorosulfonic acid; bromine; N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; methanol; water; chlorobenzene;