diamantane-4-carboxamido acetamido-isophthalic acid

Base Information

Chemical Name:diamantane-4-carboxamido acetamido-isophthalic acid
CAS No.:1379107-23-9
Molecular Formula:C₂₅H₂₈N₂O₆
Molecular Weight:452.507
Hs Code.:

Synonyms:diamantane-4-carboxamido acetamido-isophthalic acid

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Chemical Property of diamantane-4-carboxamido acetamido-isophthalic acid

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Technology Process of diamantane-4-carboxamido acetamido-isophthalic acid

There total 3 articles about diamantane-4-carboxamido acetamido-isophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1379107-18-2
diamantane-4-carboxamido acetamido-isophthalic acid dimethyl ester

: 1379107-23-9
diamantane-4-carboxamido acetamido-isophthalic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 3h;
DOI:10.1039/c2ob06915f

Reference yield:

: 1379107-07-9
2-((tert-butoxycarbonyl)amino)acetamido-isophthalic acid dimethyl ester

: 1379107-23-9
diamantane-4-carboxamido acetamido-isophthalic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 12 h / 20 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 0.17 h

2.2: 24 h / 20 °C

3.1: sodium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob06915f

Reference yield:

: 1379107-09-1
2-aminoacetamido isophthalic acid dimethyl ester trifluoroacetic acid

: 30545-18-7
MDT-17

: 1379107-23-9
diamantane-4-carboxamido acetamido-isophthalic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime / N,N-dimethyl-formamide / 0.17 h

1.2: 24 h / 20 °C

2.1: sodium hydroxide / tetrahydrofuran; methanol; water / 3 h / 20 °C

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; ethyl cyanoglyoxylate-2-oxime; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1039/c2ob06915f