C₆H₅B(OSi(CH₃)2CHCH₂)2

Base Information

• Chemical Name: C₆H₅B(OSi(CH₃)2CHCH₂)2
• CAS No.: 211937-39-2
• Molecular Formula: C₁₄H₂₃BO₂Si₂
• Molecular Weight: 290.317
• Mol file: 211937-39-2.mol

Synonyms:C₆H₅B(OSi(CH₃)2CHCH₂)2

Chemical Property of C₆H₅B(OSi(CH₃)2CHCH₂)2

Chemical Property:

Purity/Quality:

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Technology Process of C₆H₅B(OSi(CH₃)2CHCH₂)2

There total 1 articles about C₆H₅B(OSi(CH₃)2CHCH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Chlorodimethylvinylsilane (1719-58-0) + phenylboronic acid (98-80-6) → C6H5B(OSi(CH3)2CHCH2)2 (211937-39-2)

Guidance literature:

With triethylamine; In diethyl ether; byproducts: NHEt3Cl; dropwise addn. of 2 equiv. of Si-compd. to mixt. of B-compd. and Et3N at0°C, stirring (room temp., 4 h); filtration off of NHEt3Cl, evapn., distn. (vac.);

DOI:10.1016/S0022-328X(98)00498-7

Reference yield: 80.0%

C6H5B(OSi(CH3)2CHCH2)2 (211937-39-2) → (C6H5)B(OSi(CH3)2)2CCH2 (211937-46-1)

Guidance literature:

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium; In neat (no solvent); byproducts: C2H4; stirring in vac. for 18 h; distn. (vac.);

DOI:10.1016/S0022-328X(98)00498-7

upstream raw materials:

Chlorodimethylvinylsilane

phenylboronic acid

Downstream raw materials:

(C₆H₅)B(OSi(CH₃)2)2CCH₂