2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane

Base Information

• Chemical Name: 2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane
• CAS No.: 1245747-07-2
• Molecular Formula: C₁₈H₂₀F₆O₂S₃
• Molecular Weight: 478.544
• Mol file: 1245747-07-2.mol

Synonyms:2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane

Chemical Property of 2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane

There total 1 articles about 2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C13H15F6O5PS (934177-58-9) + 5-(1',3'-dithian-2'-yl)pentanal (152265-87-7) → 2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane (1245747-07-2)

Guidance literature:

C₁₃H₁₅F₆O₅PS; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

5-(1',3'-dithian-2'-yl)pentanal; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1016/j.tetasy.2010.03.043

Reference yield: 81.0%

2-[6-(3,5-bis-trifluoromethyl-phenylsulfonyl)hex-5-enyl]-[1,3]dithiane (1245747-07-2) → (E)-7-(3,5-bis-trifluoromethylphenylsulfonyl)hept-6-enal (1245747-12-9)

Guidance literature:

With calcium carbonate; methyl iodide; In water; acetonitrile; at 45 ℃; for 3h;

DOI:10.1016/j.tetasy.2010.03.043

upstream raw materials:

C₁₃H₁₅F₆O₅PS

5-(1',3'-dithian-2'-yl)pentanal

Downstream raw materials:

(E)-7-(3,5-bis-trifluoromethylphenylsulfonyl)hept-6-enal