Technology Process of 5-benzyloxy-2-(1,3-dioxan-2-yl)phenol
There total 5 articles about 5-benzyloxy-2-(1,3-dioxan-2-yl)phenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
2: tetra-N-butylammonium tribromide; trimethyl orthoformate / methanol / 2 h / 10 - 20 °C / Inert atmosphere
3: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere
With
pyridine; tetra-N-butylammonium tribromide; potassium carbonate; trimethyl orthoformate;
In
methanol; dichloromethane;
DOI:10.1016/j.tetlet.2013.05.121
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / acetonitrile / 48 h / Reflux; Inert atmosphere
2: pyridine / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere
3: tetra-N-butylammonium tribromide; trimethyl orthoformate / methanol / 2 h / 10 - 20 °C / Inert atmosphere
4: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere
With
pyridine; tetra-N-butylammonium tribromide; sodium hydrogencarbonate; potassium carbonate; trimethyl orthoformate;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2013.05.121
