2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

Base Information

Chemical Name:2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester
CAS No.:627874-38-8
Molecular Formula:C₃₆H₃₈N₆O₈
Molecular Weight:682.733
Hs Code.:

2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5<i>H</i>,10<i>H</i>-diimidazo[1,5-<i>a</i>;1',5'-<i>d</i>]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

Synonyms:2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

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Chemical Property of 2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

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Technology Process of 2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

There total 2 articles about 2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 59157-06-1
4H,9H-diimidazo<1,5-a; 1',5'-d>pyrazine-5,10-dione-1,6-dicarboxylic dichloride

: 1738-77-8
L-leucine benzyl ester p-toluenesulfonate

: 627874-38-8
2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

Guidance literature:: With N,N-diethylaniline; In dichloromethane; at -78 - 20 ℃; for 1.5h;
DOI:10.3390/molecules13123149

Reference yield: 84.0%

: 59157-06-1
4H,9H-diimidazo<1,5-a; 1',5'-d>pyrazine-5,10-dione-1,6-dicarboxylic dichloride

: 2462-35-3
L-leucine benzyl ester hydrochloride

: 627874-38-8
2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

Guidance literature:: With N,N-diethylaniline; In dichloromethane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/cc1000105

Reference yield: 97.0%

: 627874-38-8
2-{[6-(1-benzyloxycarbonyl-3-methyl-butylcarbamoyl)-5,10-dioxo-5H,10H-diimidazo[1,5-a;1',5'-d]pyrazine-1-carbonyl]-amino}-4-methyl-pentanoic acid benzyl ester

: 1738-77-8
L-leucine benzyl ester p-toluenesulfonate

: 1135306-47-6
C₃₁H₃₈N₄O₆

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.3390/molecules14010352