(R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Base Information

Chemical Name:(R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester
CAS No.:136025-93-9
Molecular Formula:C₂₀H₃₂NO₂PS₂
Molecular Weight:413.585
Hs Code.:

Synonyms:(R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

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Chemical Property of (R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

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Technology Process of (R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

There total 9 articles about (R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 110-91-8,99108-56-2
morpholine

: 129992-32-1
R_P-L-menthoxyphenylthioxaphosphoranesulfenyl chloride

: 136025-93-9
(R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Guidance literature:: In hexane; at 0 - 5 ℃;
DOI:10.1016/S0040-4020(98)00529-8

Reference yield: 99.0%

: 2958-89-6
N-(chlorosulfanyl)morpholine

: 54088-45-8,136087-28-0,136088-02-3
L(-)mentylphenylhydrogen phosphonate (S)

: 136025-93-9
(R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Guidance literature:: With triethylamine; In hexane; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00529-8

Reference yield:

: (-)-(o-menthyl)chlorophenylphosphine

: 136025-93-9
(R)-Phenyl-phosphonodithioic acid O-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester S-morpholin-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂S, pyridine

2: 99 percent / Et₃N / hexane / 1 h / Ambient temperature

With pyridine; hydrogen sulfide; triethylamine; In hexane;
DOI:10.1016/S0040-4020(98)00529-8