2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose
CAS No.:714269-56-4
Molecular Formula:C₂₉H₃₄O₉
Molecular Weight:526.584
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

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Chemical Property of 2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

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Technology Process of 2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

There total 4 articles about 2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: methyl 1-C-[3-[(4-ethylphenyl)methyl]phenyl]-2,3,4,6-tetraacetate-α-D-glucopyranoside

: 714269-56-4
2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In water; acetonitrile; at 20 ℃; for 4 - 7h;

Reference yield:

: 90-80-2,1335-57-5,4253-68-3
D-Glucono-1,5-lactone

: 714269-56-4
2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-methyl-morpholine / tetrahydrofuran / 5.75 h / 5 - 35 °C / Large scale reaction

2.1: n-butyllithium / tetrahydrofuran; hexane; toluene / -70 °C / Large scale reaction

2.2: 70 °C / Inert atmosphere

2.3: 60 °C

3.1: dmap; N-ethyl-N,N-diisopropylamine / 35 °C

4.1: triethylsilane; boron trifluoride diethyl etherate / water; acetonitrile / 0.33 h / 15 °C / Large scale reaction

With 4-methyl-morpholine; triethylsilane; dmap; n-butyllithium; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; water; toluene; acetonitrile;
DOI:10.1021/op200306q

Reference yield:

: 32469-28-6,55515-28-1,55515-29-2,32384-65-9
(3R,4S,5R,6R)-3,4,5-tris((trimethylsilyl)oxy)-6-(((trimethylsilyl)oxy)methyl)tetrahydro-2H-pyran-2-one

: 714269-56-4
2,3,4,6-tetra-O-acetyl-1-C-(4'ethyldiphenylmethan-3yl)-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane; toluene / -70 °C / Large scale reaction

1.2: 70 °C / Inert atmosphere

1.3: 60 °C

2.1: dmap; N-ethyl-N,N-diisopropylamine / 35 °C

3.1: triethylsilane; boron trifluoride diethyl etherate / water; acetonitrile / 0.33 h / 15 °C / Large scale reaction

With triethylsilane; dmap; n-butyllithium; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; water; toluene; acetonitrile;
DOI:10.1021/op200306q