4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

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Chemical Name:4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate
CAS No.:1422466-77-0
Molecular Formula:C₄₉H₆₈N₂O₃
Molecular Weight:733.091
Hs Code.:

Synonyms:4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

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Chemical Property of 4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

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Technology Process of 4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

There total 13 articles about 4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1592-20-7,29296-32-0
4-Vinylbenzyl chloride

: 1422466-93-0
4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl)benzoic acid

: 1422466-77-0
4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

Guidance literature:: 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl)benzoic acid; With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 1h; Inert atmosphere;

4-Vinylbenzyl chloride; In N,N-dimethyl-formamide; at 60 ℃; for 15h;
DOI:10.1002/chem.201202246

Reference yield:

: 1422466-81-6
methyl 2-dodecyl-4-tridecylbenzoate

: 1422466-77-0
4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / tetrahydrofuran; water; methanol / 48 h / Reflux

2.1: thionyl chloride; N,N-dimethyl-formamide / 4 h / Reflux

3.1: hydrazine hydrate / ethanol; dichloromethane / 0 - 20 °C

4.1: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

4.2: 0.5 h / Inert atmosphere

5.1: trichlorophosphate / 8 h / 85 °C

6.1: potassium hydroxide / tetrahydrofuran; water; methanol / Reflux

7.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 1 h / Inert atmosphere

7.2: 15 h / 60 °C

With thionyl chloride; sodium hydrogencarbonate; hydrazine hydrate; N,N-dimethyl-formamide; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201202246

Reference yield:

: 1422466-83-8
2-dodecyl-4-tridecylbenzohydrazide

: 1422466-77-0
4-vinylbenzyl 4-(5-(2-dodecyl-4-tridecylphenyl)-1,3,4-oxadiazol-2-yl) benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere

2.1: trichlorophosphate / 8 h / 85 °C

3.1: potassium hydroxide / tetrahydrofuran; water; methanol / Reflux

4.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 1 h / Inert atmosphere

4.2: 15 h / 60 °C

With sodium hydrogencarbonate; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201202246