(S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

Base Information

Chemical Name:(S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide
CAS No.:771489-11-3
Molecular Formula:C₂₃H₄₄N₂O₃
Molecular Weight:396.614
Hs Code.:

Synonyms:(S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

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Chemical Property of (S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

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Technology Process of (S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

There total 5 articles about (S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: <4S-(4R*,5S*,6R*)>-6-(Boc-amino)-2-methyl-11-phenylundecane-4,5-diol

: 771489-11-3
(S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / hydrogen / 10percent Rh/C / propan-2-ol / 25 °C / 2585.7 Torr

2: 85.4 percent / HCl gas / CH₂Cl₂ / 3.5 h

3: 77.8 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide

4: 1.) HCl gas, 2.) sodium bicarbonate / 1.) CH₂Cl₂, RT, 4 h, 2.) EtOAc

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; Rh on carbon; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jm00015a012

Reference yield:

: 90600-20-7
(2S)-2-[(tert-butoxycarbonyl)amino]pent-4-enoic acid

: 771489-11-3
(S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 77.8 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide

2: 1.) HCl gas, 2.) sodium bicarbonate / 1.) CH₂Cl₂, RT, 4 h, 2.) EtOAc

With hydrogenchloride; sodium hydrogencarbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00015a012

Reference yield:

: 167113-52-2
<4S-(4R*,5S*,6R*)>-6-amino-11-cyclohexyl-2-methylundecane-4,5-diol

: 771489-11-3
(S)-2-Amino-pent-4-enoic acid [(1S,2R,3S)-1-(5-cyclohexyl-pentyl)-2,3-dihydroxy-5-methyl-hexyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 77.8 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodiimide / dimethylformamide

2: 1.) HCl gas, 2.) sodium bicarbonate / 1.) CH₂Cl₂, RT, 4 h, 2.) EtOAc

With hydrogenchloride; sodium hydrogencarbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1021/jm00015a012