Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester

Base Information

• Chemical Name: Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester
• CAS No.: 193952-85-1
• Molecular Formula: C₅₄H₆₀O₁₈
• Molecular Weight: 997.06

Synonyms:Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester

Chemical Property of Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester

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Technology Process of Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester

There total 1 articles about Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.6%

1,3,5-benzene tris(carbonyl chloride) (4422-95-1) + (R)-(-)-2-benzyloxycarbonyl-1-methylethyl (R)-(-)-3-hydroxybutyrate (101515-40-6) → Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester (193952-85-1)

Guidance literature:

With pyridine; In dichloromethane; for 27h; Ambient temperature;

DOI:10.1002/hlca.19970800402

Reference yield: 98.0%

1,2-dichloro-ethane (107-06-2,52399-93-6) + Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester (193952-85-1) → Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-carboxy-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester; compound with 1,2-dichloro-ethane

Guidance literature:

With hydrogen; palladium on activated charcoal; In various solvent(s);

DOI:10.1002/hlca.19970800402

Reference yield:

Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-benzyloxycarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester (193952-85-1) → Benzene-1,3,5-tricarboxylic acid tris-[(R)-2-((R)-2-chlorocarbonyl-1-methyl-ethoxycarbonyl)-1-methyl-ethyl] ester

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / H₂ / 10 percent Pd/C / various solvent(s)

2: oxalyl chloride / CH₂Cl₂ / Ambient temperature

With oxalyl dichloride; hydrogen; palladium on activated charcoal; In dichloromethane;

DOI:10.1002/hlca.19970800402

upstream raw materials:

1,3,5-benzene tris(carbonyl chloride)

(R)-(-)-2-benzyloxycarbonyl-1-methylethyl (R)-(-)-3-hydroxybutyrate

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