decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Base Information

Chemical Name:decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside
CAS No.:173314-36-8
Molecular Formula:C₅₃H₇₆O₂₅
Molecular Weight:1113.17
Hs Code.:

Synonyms:decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Chemical Property of decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

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Technology Process of decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

There total 8 articles about decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 108-24-7
acetic anhydride

: 173314-34-6
decyl O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

: Acetic acid (2R,3R,4S,5R,6S)-3-acetoxy-2-acetoxymethyl-6-decyloxy-5-((2R,3R,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

: 173314-36-8
decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: With pyridine; dmap; 3,4,6-tri-O-acetyl-2-O-benzyl-β-D-glucopyranosyl chloride; 4 A molecular sieve; silver perchlorate; silver carbonate; In dichloromethane; at 22 ℃; for 24h;
DOI:10.1016/0008-6215(95)00199-4

Reference yield:

: 29741-67-1
1,3,4,6-tetra-O-acetyl-2-O-benzyl-β-D-glucopyranoside

: 173314-36-8
decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 64 h / Heating

2: 76 percent / Cl₂ / CH₂Cl₂; CCl₄ / 0.25 h / 22 °C

3: 1.) Ag₂CO₃, 4A molecular sieves, 2.) AgClO₄ / 1.) CH₂Cl₂, 22 deg C, 2 h, 2.) CH₂Cl₂, 22 deg C, 48 h

4: 85 percent / H₂, AcOH / Pd/C / ethanol / 14 h / 22 °C / 2587.7 Torr

5: 1.) Ag₂CO₃, 4A molecular sieves, 2.) AgClO₄ / 1.) CH₂Cl₂, 22 deg C, 1 h, 2.) CH₂Cl₂, 22 deg C, 36 h

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; hydrogen; silver perchlorate; chlorine; acetic acid; silver carbonate; palladium on activated charcoal; In tetrachloromethane; ethanol; dichloromethane;
DOI:10.1016/0008-6215(95)00199-4

Reference yield:

: 173314-28-8
phenyl 3,4,6-tri-O-acetyl-2-O-benzyl-1-thio-α-D-glucopyranoside

: 173314-36-8
decyl O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-(1<*>2)-O-(3,4,6-tri-O-acetyl-α-D-glucopyranosyl)-(1<*>2)-3,4,6-tri-O-acetyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / Cl₂ / CH₂Cl₂; CCl₄ / 0.25 h / 22 °C

2: 1.) Ag₂CO₃, 4A molecular sieves, 2.) AgClO₄ / 1.) CH₂Cl₂, 22 deg C, 2 h, 2.) CH₂Cl₂, 22 deg C, 48 h

3: 85 percent / H₂, AcOH / Pd/C / ethanol / 14 h / 22 °C / 2587.7 Torr

4: 1.) Ag₂CO₃, 4A molecular sieves, 2.) AgClO₄ / 1.) CH₂Cl₂, 22 deg C, 1 h, 2.) CH₂Cl₂, 22 deg C, 36 h

With 4 A molecular sieve; hydrogen; silver perchlorate; chlorine; acetic acid; silver carbonate; palladium on activated charcoal; In tetrachloromethane; ethanol; dichloromethane;
DOI:10.1016/0008-6215(95)00199-4