3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate

Base Information

• Chemical Name: 3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate
• CAS No.: 1146216-58-1
• Molecular Formula: C₁₃H₁₄N₂O₃
• Molecular Weight: 246.266
• Mol file: 1146216-58-1.mol

Synonyms:3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate

Chemical Property of 3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate

There total 1 articles about 3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3-hydroxy-3-methyl-1-cyano-1-butyne (32837-87-9) + meta-aminobenzoic acid (99-05-8,159139-79-4) → 3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate (1146216-58-1)

Guidance literature:

In acetonitrile; at 20 - 75 ℃; regiospecific reaction;

DOI:10.1016/j.tet.2009.01.073

Reference yield:

3-cyano-1,1-dimethyl-2-oxopropyl 3-aminobenzenecarboxylate (1146216-58-1) → C13H12N2O2

Guidance literature:

at 250 ℃;

DOI:10.1016/j.tet.2009.01.073

upstream raw materials:

3-hydroxy-3-methyl-1-cyano-1-butyne

meta-aminobenzoic acid