(+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate

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Chemical Name:(+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate
CAS No.:82338-55-4
Molecular Formula:C₄₁H₄₀ClOP₄Ru*F₆P
Molecular Weight:954.15
Hs Code.:

Synonyms:(+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate

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Chemical Property of (+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate

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Technology Process of (+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate

There total 2 articles about (+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: ammonium hexafluorophosphate

: 82373-48-6
(+)589-λ-anti-cis-C2-dichlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II)

: 82338-55-4
(+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate

Guidance literature:: With CO; In ethanol; CO passed into boiling suspn. of Ru complex in ethanol for 15 min, excess of aq. NH4PF6 soln. slowly added to mixt.; ppt. filtered off, washed with water, dried, recrystd. from acetone by addn. of diethyl ether;

Reference yield: 86.0%

: ammonium hexafluorophosphate

: 72091-01-1,72091-02-2,72150-36-8,72150-63-1,77410-05-0
(R,R)-1,2-bis(methylphenylphosphino)benzene

: 82373-39-5,82373-36-2,82373-34-0,82338-43-0
trans-dicarbonyldichlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II)

: 82338-55-4
(+)589-λ-anti-cis-C1-carbonylchlorobis((S,S)-o-phenylenebis(methylphenylphosphine))ruthenium(II) hexafluorophosphate

Guidance literature:: In ethanol; suspn. of Ru complex and ligand in ethanol refluxed for 40 min, added aq. NH4PF6; ppt. filtered, recrystd. from acetone by addn. of diethyl ether;