{(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

Base Information

Chemical Name:{(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester
CAS No.:1221593-56-1
Molecular Formula:C₂₄H₃₈N₄O₆
Molecular Weight:478.589
Hs Code.:

Synonyms:{(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

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Chemical Property of {(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

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Technology Process of {(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

There total 7 articles about {(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1221593-55-0
{(S)-5-amino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethylcarbamoyl]-pentyl}-carbamic acid tert-butyl ester

: 108-24-7
acetic anhydride

: 1221593-56-1
{(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; at 20 ℃; for 2h;

Reference yield: 99.0%

: 1221593-55-0
{(S)-5-amino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethylcarbamoyl]-pentyl}-carbamic acid tert-butyl ester

: 1221593-56-1
{(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In chloroform; ethyl acetate; at 20 ℃; for 2h;

Reference yield:

: 71989-26-9
Fmoc-Lys(tert-butoxycarbonyl)

: 1221593-56-1
{(S)-5-acetylamino-5-[2-(benzyloxycarbonyl-methyl-amino)-ethyl carbamoyl]-pentyl}-carbamic acid isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 5 °C

1.3: 2 h / 20 °C

2.1: piperidine / ethyl acetate / 18 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / chloroform / 2 h / 20 °C

With piperidine; N-ethyl-N,N-diisopropylamine; In chloroform; ethyl acetate; N,N-dimethyl-formamide;