Technology Process of C51H38O2S4
There total 4 articles about C51H38O2S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; potassium hydroxide;
In
tetrahydrofuran;
at 80 ℃;
for 6h;
DOI:10.1002/chem.201003627
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 7 h / -78 - 20 °C / Inert atmosphere
1.2: 48 h / 100 °C / Inert atmosphere
2.1: water; potassium hydroxide / tetrahydrofuran / 6 h / 80 °C
With
n-butyllithium; water; potassium hydroxide;
In
tetrahydrofuran; hexane;
1.2: Stille coupling;
DOI:10.1002/chem.201003627
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium
1.2: 48 h / 100 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 7 h / -78 - 20 °C / Inert atmosphere
2.2: 48 h / 100 °C / Inert atmosphere
3.1: water; potassium hydroxide / tetrahydrofuran / 6 h / 80 °C
With
n-butyllithium; water; potassium hydroxide;
In
tetrahydrofuran; hexane;
1.2: Stille coupling / 2.2: Stille coupling;
DOI:10.1002/chem.201003627