N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

Base Information

Chemical Name:N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone
CAS No.:151919-84-5
Molecular Formula:C₂₅H₃₃NO₇
Molecular Weight:459.54
Hs Code.:

Synonyms:N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

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Chemical Property of N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

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Technology Process of N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

There total 3 articles about N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 151919-83-4
N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydroisoquinoline

: 151919-84-5
N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

Guidance literature:: With potassium permanganate; magnesium sulfate; In water; acetone; for 0.333333h; Ambient temperature;

Reference yield:

: 5471-40-9
3,4,3',4'-tetramethoxy-bibenzyl-α-ylamine

: 151919-84-5
N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 1 M aq. HCl / 50 °C

2: 88 percent / KOH / dimethylsulfoxide / 4 h / 80 °C

3: 65 percent / KMnO₄, MgSO₄ / acetone; H₂O / 0.33 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; potassium permanganate; magnesium sulfate; In water; dimethyl sulfoxide; acetone;

Reference yield:

: 33329-41-8
6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-1,2,3,4-tetrahydroisoquinoline

: 151919-84-5
N-(2,2-diethoxyethyl)-6,7-dimethoxy-3-(3,4-dimethoxyphenyl)-3,4-dihydro-1(2H)-isoquinolinone

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / KOH / dimethylsulfoxide / 4 h / 80 °C

2: 65 percent / KMnO₄, MgSO₄ / acetone; H₂O / 0.33 h / Ambient temperature

With potassium hydroxide; potassium permanganate; magnesium sulfate; In water; dimethyl sulfoxide; acetone;