2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside
CAS No.:865488-96-6
Molecular Formula:C₄₆H₆₀INO₂₅
Molecular Weight:1153.88
Hs Code.:

2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Synonyms:2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

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Chemical Property of 2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

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Technology Process of 2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

There total 27 articles about 2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 865488-94-4
2-(4-iodophenyl)ethyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

: 1357000-53-3
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-1-thio-α-D-mannopyranoside

: 865488-96-6
2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -50 ℃; for 2.5h; Molecular sieve;
DOI:10.3987/COM-11-12332

Reference yield: 67.0%

: 865488-94-4
2-(4-iodophenyl)ethyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

: 126777-59-1
2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl bromide

: 865488-96-6
2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With silver perchlorate; silver carbonate; In dichloromethane; toluene; for 15h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.05.047

Reference yield:

: 865488-85-3
C₃₄H₄₃NO₁₄

: 865488-96-6
2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / 20 °C

2: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 50 °C / 760.05 Torr

3: pyridine / 20 °C

4: hydrogen bromide; acetic anhydride; acetic acid / 20 °C / Inert atmosphere

5: silver perchlorate; silver carbonate / dichloromethane; toluene / 15 h / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen bromide; hydrogen; silver perchlorate; acetic anhydride; acetic acid; silver carbonate; In ethanol; dichloromethane; toluene;
DOI:10.1016/j.bmc.2011.05.047