Technology Process of C49H70N6O11
There total 12 articles about C49H70N6O11 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: potassium carbonate / 5 h / 20 °C
2.1: sodium tetrahydroborate / methanol / 5 h / 0 - 20 °C
3.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere
4.1: methanol; tetrahydrofuran / 0.25 h / 0 - 20 °C
4.2: 12 h / 0 - 20 °C / Inert atmosphere
5.1: dmap; triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
6.1: palladium 10% on activated carbon; ammonia / methanol / 1 h / 20 °C / Inert atmosphere
7.1: triethylamine / tetrahydrofuran / 16 h / 20 °C
8.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / Inert atmosphere
With
dmap; sodium tetrahydroborate; palladium 10% on activated carbon; ammonia; hydrogen; potassium carbonate; Dess-Martin periodane; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol; tetrahydrofuran / 0.25 h / 0 - 20 °C
1.2: 12 h / 0 - 20 °C / Inert atmosphere
2.1: dmap; triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; ammonia / methanol / 1 h / 20 °C / Inert atmosphere
4.1: triethylamine / tetrahydrofuran / 16 h / 20 °C
5.1: palladium 10% on activated carbon; hydrogen / methanol / 1 h / Inert atmosphere
With
dmap; palladium 10% on activated carbon; ammonia; hydrogen; triethylamine;
In
tetrahydrofuran; methanol;