tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

Base Information

Chemical Name:tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate
CAS No.:1237518-47-6
Molecular Formula:C₂₉H₃₁BrN₂O₅
Molecular Weight:567.48
Hs Code.:

Synonyms:tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

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Chemical Property of tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

Chemical Property:

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Technology Process of tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

There total 4 articles about tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 890315-73-8
tert-butyl 2-amino-4-bromobenzoate

: 2-(benzyloxy)-5-(morpholin-4-yl)benzoic acid chloride

: 1237518-47-6
tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

Guidance literature:: With pyridine; In tetrahydrofuran; at 20 - 50 ℃; for 1h;

Reference yield:

: 5-amino-2-benzyloxybenzoic acid methyl ester

: 1237518-47-6
tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; potassium iodide / ISOPROPYLAMIDE / 3 h / 100 °C

2: sodium hydroxide; water / ethanol / 1 h / 50 °C

3: oxalyl dichloride / N,N-dimethyl-formamide / tetrahydrofuran / 2.17 h / 20 °C / Reflux

4: pyridine / tetrahydrofuran / 1 h / 20 - 50 °C

With pyridine; oxalyl dichloride; water; potassium carbonate; potassium iodide; sodium hydroxide; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; ISOPROPYLAMIDE;

Reference yield:

: 1237518-46-5
2-(benzyloxy)-5-(morpholin-4-yl)benzoic acid

: 1237518-47-6
tert-butyl 2-(2-(benzyloxy)-5-(morpholin-4-yl)benzamido)-4-bromobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / tetrahydrofuran / 2.17 h / 20 °C / Reflux

2: pyridine / tetrahydrofuran / 1 h / 20 - 50 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran;