C₆₈H₉₁ClN₂O₁₉

Base Information

Chemical Name:C₆₈H₉₁ClN₂O₁₉
CAS No.:869317-87-3
Molecular Formula:C₆₈H₉₁ClN₂O₁₉
Molecular Weight:1275.93
Hs Code.:

C<sub>68</sub>H<sub>91</sub>ClN<sub>2</sub>O<sub>19</sub>

Synonyms:C₆₈H₉₁ClN₂O₁₉

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Chemical Property of C₆₈H₉₁ClN₂O₁₉

Chemical Property:

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Technology Process of C₆₈H₉₁ClN₂O₁₉

There total 1 articles about C₆₈H₉₁ClN₂O₁₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₆₀H₈₅ClN₂O₁₇

: 530-62-1
1,1'-carbonyldiimidazole

: 100-51-6,185532-71-2
benzyl alcohol

: 869317-87-3
C₆₈H₉₁ClN₂O₁₉

Guidance literature:: C₆₀H₈₅ClN₂O₁₇; 1,1'-carbonyldiimidazole; With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 2h;

benzyl alcohol; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: 869317-87-3
C₆₈H₉₁ClN₂O₁₉

: 869317-91-9
C₅₃H₆₇ClF₂N₂O₁₄

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / NaH; MeI / 4.5 h / 60 °C

2: 63 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 72 h / 20 °C

3: 88 percent / hydrochloric acid / methanol / 1.5 h / 50 °C

4: 89 percent / DMSO; (CF₃CO)2O; Et₃N / CH₂Cl₂ / 1 h / -78 °C

With hydrogenchloride; diethylamino-sulfur trifluoride; sodium hydride; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; methyl iodide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: 869317-87-3
C₆₈H₉₁ClN₂O₁₉

: 869317-90-8
C₅₃H₆₉ClF₂N₂O₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / NaH; MeI / 4.5 h / 60 °C

2: 63 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 72 h / 20 °C

3: 88 percent / hydrochloric acid / methanol / 1.5 h / 50 °C

With hydrogenchloride; diethylamino-sulfur trifluoride; sodium hydride; methyl iodide; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2005.06.003