(R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

Base Information

Chemical Name:(R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester
CAS No.:945635-08-5
Molecular Formula:C₂₆H₃₃NO₄Si
Molecular Weight:451.638
Hs Code.:

Synonyms:(R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

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Chemical Property of (R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

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Technology Process of (R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

There total 3 articles about (R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 945635-00-7
(R)-4-[tert-butyl(diphenyl)silanyloxy]pyrrolidin-2-one

: 945635-05-2
1-ethylallyl chloroformate

: 945635-08-5
(R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

Guidance literature:: With dmap; triethylamine; In acetonitrile; at 80 ℃; for 16h;
DOI:10.1021/jo070732a

Reference yield:

: 616-25-1
1-Penten-3-ol

: 945635-08-5
(R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂CO₃ / pentane / 16 h / 25 °C

2: 36 percent / Et₃N; DMAP / acetonitrile / 16 h / 80 °C

With dmap; sodium carbonate; triethylamine; In acetonitrile; pentane;
DOI:10.1021/jo070732a

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 945635-08-5
(R)-4-[tert-butyl(diphenyl)silanyloxy]-2-oxopyrrolidine-1-carboxylic acid 1-ethylallyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / imidazole / dimethylformamide / 0.5 h / 0 °C

2: 36 percent / Et₃N; DMAP / acetonitrile / 16 h / 80 °C

With 1H-imidazole; dmap; triethylamine; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo070732a