1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

Base Information

Chemical Name:1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene
CAS No.:225517-51-1
Molecular Formula:C₂₃H₂₁BrO₇
Molecular Weight:489.32
Hs Code.:

Synonyms:1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

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Chemical Property of 1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

Chemical Property:

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Technology Process of 1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

There total 4 articles about 1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3-bromo-4,5-dimethoxy-phenyl)-5-methoxy-11-oxa-tricyclo[6.2.1.0^2,7]undeca-2,4,6-triene-9,10-dicarboxylic acid dimethyl ester

: 225517-51-1
1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

Guidance literature:: With trifluoroacetic acid; In toluene; Yield given; Ambient temperature;
DOI:10.1021/jm9807048

Reference yield:

: 6948-30-7
5-bromoveratralaldehyde

: 225517-51-1
1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 30 min

2: AcOH / toluene / 2 h / Heating

3: TFA / toluene / Ambient temperature

With n-butyllithium; acetic acid; trifluoroacetic acid; In toluene;
DOI:10.1021/jm9807048

Reference yield:

: 181780-66-5
1-bromo-2-(dimethoxymethyl)-4-methoxybenzene

: 225517-51-1
1-(3-bromo-4,5-dimethoxyphenyl)-2,3-bis(methoxycarbonyl)-6-methoxynaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 30 min, 2.) THF, -78 deg C, 30 min

2: AcOH / toluene / 2 h / Heating

3: TFA / toluene / Ambient temperature

With n-butyllithium; acetic acid; trifluoroacetic acid; In toluene;
DOI:10.1021/jm9807048