3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

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Chemical Name:3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester
CAS No.:477197-72-1
Molecular Formula:C₆₁H₉₃NO₇
Molecular Weight:952.412
Hs Code.:

Synonyms:3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

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Chemical Property of 3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

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Technology Process of 3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

There total 8 articles about 3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 22355-63-1
4-[[(4-methylphenyl)methylene]amino]phenol

: 3,4-bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid

: 477197-72-1
3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1016/S0040-4039(02)01101-2

Reference yield:

: 99-24-1
methyl galloate

: 477197-72-1
3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 24 percent / NaH; KI / dimethylformamide / 60 °C

2: 63 percent / K₂CO₃ / acetonitrile / Heating

3: 83 percent / KOH / Saponification

4: 88 percent / pyridine / CH₂Cl₂ / 20 °C

5: pyridine; aq. HCl / 100 °C

6: 90 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; dimethylaminopyridine / CH₂Cl₂ / 20 °C

With pyridine; hydrogenchloride; dmap; potassium hydroxide; sodium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(02)01101-2

Reference yield:

: 143-15-7
1-dodecylbromide

: 477197-72-1
3,4-Bis-dodecyloxy-5-[12-(2-methyl-acryloyloxy)-dodecyloxy]-benzoic acid 4-{[1-p-tolyl-meth-(E)-ylidene]-amino}-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 24 percent / NaH; KI / dimethylformamide / 60 °C

2: 63 percent / K₂CO₃ / acetonitrile / Heating

3: 83 percent / KOH / Saponification

4: 88 percent / pyridine / CH₂Cl₂ / 20 °C

5: pyridine; aq. HCl / 100 °C

6: 90 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; dimethylaminopyridine / CH₂Cl₂ / 20 °C

With pyridine; hydrogenchloride; dmap; potassium hydroxide; sodium hydride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium iodide; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4039(02)01101-2