3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione

Base Information

• Chemical Name: 3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione
• CAS No.: 1257063-13-0
• Molecular Formula: C₁₃H₁₀BrN₅O₂
• Molecular Weight: 348.159

Synonyms:3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione

Chemical Property of 3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione

Chemical Property:

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Technology Process of 3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione

There total 1 articles about 3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

C13H13BrN4O2 (68871-25-0) → 3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione (1257063-13-0)

Guidance literature:

With acetic acid; sodium nitrite; In water; at 5 - 20 ℃; for 18h;

DOI:10.1016/j.tetlet.2010.09.044

Reference yield: 58.0%

3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione (1257063-13-0) → 3-(4-bromophenyl)-1,5-dimethyl-1H-imidazo[4,5-e][1,2,4]triazin-6(5H)-one

Guidance literature:

3-(4-bromophenyl)-1,6-dimethylpyrimido[5,4-e][1,2,4]triazine-5,7(1H,6H)-dione; With water; sodium hydroxide; at 60 - 70 ℃;

With hydrogenchloride; In water; pH=7; Cooling with ice;

DOI:10.1071/CH14425

upstream raw materials:

C₁₃H₁₃BrN₄O₂

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