[(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4

Base Information

Chemical Name:[(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4
CAS No.:178757-32-9
Molecular Formula:C₃₅H₃₇ClIrP₂S₂*ClO₄
Molecular Weight:910.882
Hs Code.:

Synonyms:[(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4

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Chemical Property of [(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4

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Technology Process of [(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4

There total 1 articles about [(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 12354-84-6,12354-85-7
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]

: 14633-92-2
bis(diphenylthiophosphoryl)methane

: sodium perchlorate

: 178757-32-9
[(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4

Guidance literature:: In acetone; N2-atmosphere; refluxing Ir-complex with 2 equiv. of ligand and 2 equiv.NaClO4 for 2 h; evapn., extn. into CHCl3, crystn. on hexane addn.; elem. anal.;
DOI:10.1016/0022-328X(95)05909-9

Reference yield: 79.0%

: 178757-32-9
[(η(5)-pentamethylcyclopentadienyl)IrCl(η(2)-Ph2P(S)CH2P(S)Ph2-S,S')]ClO4

: 178757-37-4
[(η(5)-pentamethylcyclopentadienyl)Ir(η(3)-Ph2P(S)CHP(S)Ph2-C,S,S')]ClO4

Guidance literature:: With thallium pyrazolate; In dichloromethane; byproducts: TlCl; N2-atmosphere; stirring equimolar amts. of Ir-complex and Tl-pyrazolate (room temp., 2 h); filtration off of TlCl (cellulose), evapn., extn. into Me2CO, addn. of Et2O, crystn. (-20°C); elem. anal.;
DOI:10.1016/0022-328X(95)05909-9