C₂₂H₁₈N₂O₆S

Base Information

Chemical Name:C₂₂H₁₈N₂O₆S
CAS No.:1428332-95-9
Molecular Formula:C₂₂H₁₈N₂O₆S
Molecular Weight:438.461
Hs Code.:

C<sub>22</sub>H<sub>18</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:C₂₂H₁₈N₂O₆S

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Chemical Property of C₂₂H₁₈N₂O₆S

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Technology Process of C₂₂H₁₈N₂O₆S

There total 7 articles about C₂₂H₁₈N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1428332-93-7
C₂₆H₂₂N₂O₈S

: 1428332-95-9
C₂₂H₁₈N₂O₆S

Guidance literature:: With hydrogenchloride; In acetone; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2013.02.011

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 1428332-95-9
C₂₂H₁₈N₂O₆S

Guidance literature:: Multi-step reaction with 7 steps

1: nitric acid; sulfuric acid / 16 h / 5 - 20 °C

2: water / 3 h / Reflux

3: nitric acid; sulfuric acid / 7 h / 20 °C

4: 3 h / Reflux

5: palladium on activated charcoal; ammonium formate / tetrahydrofuran / 12 h / 20 °C

6: triethylamine / N,N-dimethyl-formamide / 6 h / 20 °C

7: hydrogenchloride / acetone / 1 h / 20 °C

With hydrogenchloride; sulfuric acid; palladium on activated charcoal; nitric acid; ammonium formate; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2013.02.011

Reference yield:

: 89-40-7
4-nitrophthalimide

: 1428332-95-9
C₂₂H₁₈N₂O₆S

Guidance literature:: Multi-step reaction with 6 steps

1: water / 3 h / Reflux

2: nitric acid; sulfuric acid / 7 h / 20 °C

3: 3 h / Reflux

4: palladium on activated charcoal; ammonium formate / tetrahydrofuran / 12 h / 20 °C

5: triethylamine / N,N-dimethyl-formamide / 6 h / 20 °C

6: hydrogenchloride / acetone / 1 h / 20 °C

With hydrogenchloride; sulfuric acid; palladium on activated charcoal; nitric acid; ammonium formate; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmcl.2013.02.011