endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

Base Information

Chemical Name:endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene
CAS No.:660437-52-5
Molecular Formula:C₂₂H₂₂N₂O₂
Molecular Weight:346.429
Hs Code.:

endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0<sup>2,6</sup>]dec-8-ene

Synonyms:endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

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Chemical Property of endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

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Technology Process of endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

There total 3 articles about endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 660437-51-4
4-ethylenedioxy-3,5-diphenyl-4H-pyrazol

: 660437-52-5
endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

Guidance literature:: cyclopenta-1,3-diene; 4-ethylenedioxy-3,5-diphenyl-4H-pyrazol;

With hydrogen; palladium on activated charcoal;
DOI:10.1021/ja038305b

Reference yield:

: 643-75-4
1,3-diphenyl-propane-1,2,3-trione

: 660437-52-5
endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

Guidance literature:: Multi-step reaction with 3 steps

1.1: 65 percent / K₂CO₃ / tetrahydrofuran; dimethylsulfoxide / 24 h / 40 °C

2.1: NH₂NH₂*H₂O / CHCl₃ / 24 h / Heating

3.2: 35 percent / H₂ / Pd/C

With potassium carbonate; hydrazine hydrate; In tetrahydrofuran; chloroform; dimethyl sulfoxide;
DOI:10.1021/ja038305b

Reference yield:

: 660437-50-3
1,3-diphenyl-2-ethylenedioxypropane-1,3-dione

: 660437-52-5
endo-10,10-ethylenedioxy-1,7-diphenyl-8,9-diazatricyclo[5.2.1.0^2,6]dec-8-ene

Guidance literature:: Multi-step reaction with 2 steps

1.1: NH₂NH₂*H₂O / CHCl₃ / 24 h / Heating

2.2: 35 percent / H₂ / Pd/C

With hydrazine hydrate; In chloroform;
DOI:10.1021/ja038305b