methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate

Base Information

Chemical Name:methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate
CAS No.:1100708-12-0
Molecular Formula:C₂₆H₂₂N₂O₃
Molecular Weight:410.472
Hs Code.:

Synonyms:methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate

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Technology Process of methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate

There total 1 articles about methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 81000-30-8
2,4-dihydro-5-methyl-2-phenyl-4-(diphenylmethylene)-3H-pyrazol-3-one

: 96-34-4
methyl chloroacetate

: 1100708-12-0
methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 5 ℃; for 2h;
DOI:10.1002/jhet.5570450653

Reference yield: 99.0%

: 1100708-12-0
methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate

: 1187037-51-9
methyl 2-(5-methyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-3,3-diphenylacrylate

Guidance literature:: methyl 5,6-diaza-4-methyl-7-oxo-2,2,6-triphenylsipro[2,4]hept-4-ene-1-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

With hydrogenchloride; In water; N,N-dimethyl-formamide; Cooling with ice;
DOI:10.1002/jhet.117