3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

Base Information

Chemical Name:3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide
CAS No.:227289-22-7
Molecular Formula:C₁₃H₁₉N₃O₃
Molecular Weight:265.312
Hs Code.:

3-<N<sup>1</sup>-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

Synonyms:3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

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Chemical Property of 3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

Chemical Property:

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Technology Process of 3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

There total 2 articles about 3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 107746-30-5
3-hydrazino-N,N-(dimethyl)propanamide

: 227289-22-7
3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

: 255873-55-3
3-[N¹,N²-bis(carbobenzyloxy)hydrazino]-N,N-dimethylpropanamide

Guidance literature:: With sodium hydroxide; In diethyl ether; at 0 - 5 ℃; for 1h;
DOI:10.1016/S0968-0896(99)00006-1

Reference yield:

: 2680-03-7,68761-83-1
N,N-Dimethylacrylamide

: 227289-22-7
3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 6.5 g / hydrazine monohydrate / methanol / 2 h / Ambient temperature

2: 30 percent / aq. NaOH / diethyl ether / 1 h / 0 - 5 °C

With sodium hydroxide; hydrazine hydrate; In methanol; diethyl ether;
DOI:10.1016/S0968-0896(99)00006-1

Reference yield: 76.0%

: Ac-Leu-Ala-Ala-OH

: 227289-22-7
3-1-(benzyloxycarbonyl)hydrazino>-N,N-(dimethyl)propanamide

: 227289-23-8
3-1-(benzyloxycarbonyl)-N²-(acetyl-L-leucyl-L-alanyl-L-alanyl)hydrazino>-N,N-(dimethyl)propanamide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; for 6h; Ambient temperature;
DOI:10.1016/S0968-0896(99)00006-1