N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

Base Information

Chemical Name:N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide
CAS No.:80976-40-5
Molecular Formula:C₂₇H₁₉N₃O₇S₂
Molecular Weight:561.596
Hs Code.:

Synonyms:N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

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Technology Process of N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

There total 11 articles about N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 80964-17-6
N-hydroxy-1H-naphth<2,3-d>imidazole-6,7-dicarboximide

: 98-59-9
p-toluenesulfonyl chloride

: 80976-40-5
N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

Guidance literature:: With 4-amino-2,3-dimethylpyridine; In pyridine; dimethyl sulfoxide; for 1.5h;
DOI:10.1021/ja00373a046

Reference yield:

: 4082-23-9
3-amino-4-nitrobicyclo<4.2.0>octa-1,3,5-triene

: 80976-40-5
N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

Guidance literature:: Multi-step reaction with 8 steps

1: 65 percent / 0.17 h / Heating

3: 91 percent / HCl / methanol / 2.5 h / Heating

4: H₂ / 10percent Pd/C / methanol / 2 h

5: 2 N NaOH / methanol / 0.5 h / Heating

6: 77 percent / 1 h / Heating

7: 96 percent / NH₂OH*HCl / pyridine / 12 h / 80 °C

8: 72 percent / dimethyl-4-aminopyridine / pyridine; dimethylsulfoxide / 1.5 h

With hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; hydrogen; 4-amino-2,3-dimethylpyridine; palladium on activated charcoal; In pyridine; methanol; dimethyl sulfoxide;
DOI:10.1021/ja00373a046

Reference yield:

: 4082-21-7
3-acetamido-4-nitrobicyclo<4.2.0>octa-1,3,5-triene

: 80976-40-5
N-p-(tolylsulfonoxy)-1-p-(tolylsulfonyl)naphth<2,3-d>imidazole-6,7-dicarboximide

Guidance literature:: Multi-step reaction with 7 steps

2: 91 percent / HCl / methanol / 2.5 h / Heating

3: H₂ / 10percent Pd/C / methanol / 2 h

4: 2 N NaOH / methanol / 0.5 h / Heating

5: 77 percent / 1 h / Heating

6: 96 percent / NH₂OH*HCl / pyridine / 12 h / 80 °C

7: 72 percent / dimethyl-4-aminopyridine / pyridine; dimethylsulfoxide / 1.5 h

With hydrogenchloride; sodium hydroxide; hydroxylamine hydrochloride; hydrogen; 4-amino-2,3-dimethylpyridine; palladium on activated charcoal; In pyridine; methanol; dimethyl sulfoxide;
DOI:10.1021/ja00373a046