3,4-dichlorophenylsulfur pentafluoride

Base Information

• Chemical Name: 3,4-dichlorophenylsulfur pentafluoride
• CAS No.: 165114-86-3
• Molecular Formula: C₆H₃Cl₂F₅S
• Molecular Weight: 273.054
• Mol file: 165114-86-3.mol

Synonyms:3,4-dichlorophenylsulfur pentafluoride

Chemical Property of 3,4-dichlorophenylsulfur pentafluoride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-dichlorophenylsulfur pentafluoride

There total 3 articles about 3,4-dichlorophenylsulfur pentafluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

2-chloro-4-(pentafluoro-λ6-sulfanyl)aniline (165114-85-2) → 3,4-dichlorophenylsulfur pentafluoride (165114-86-3)

Guidance literature:

2-chloro-4-(pentafluoro-λ⁶-sulfanyl)aniline; With tert.-butylnitrite; copper dichloride; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;

With hydrogenchloride; In water; acetonitrile;

Reference yield:

1-nitro-4-(pentafluorosulfanyl)benzene (2613-27-6) → 3,4-dichlorophenylsulfur pentafluoride (165114-86-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 99 percent / H₂ / Raney nickel / ethanol

2: NCS / acetonitrile

3: t-BuONO; CuCl₂ / acetonitrile

With N-chloro-succinimide; tert.-butylnitrite; hydrogen; copper dichloride; nickel; In ethanol; acetonitrile;

DOI:10.2533/000942904777678172

Reference yield:

4-(pentafluorosulfanyl)aniline (2993-24-0) → 3,4-dichlorophenylsulfur pentafluoride (165114-86-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NCS / acetonitrile

2: t-BuONO; CuCl₂ / acetonitrile

With N-chloro-succinimide; tert.-butylnitrite; copper dichloride; In acetonitrile;

DOI:10.2533/000942904777678172

upstream raw materials:

2-chloro-4-(pentafluoro-λ⁶-sulfanyl)aniline

1-nitro-4-(pentafluorosulfanyl)benzene

4-(pentafluorosulfanyl)aniline

Downstream raw materials:

C₁₃H₈ClF₅O₃S

C₁₃H₇ClF₅NO₅S

C₁₄H₉ClF₅NO₅S

C₁₄H₁₀ClF₅O₃S