1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

Base Information

Chemical Name:1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone
CAS No.:117320-70-4
Molecular Formula:C₁₆H₁₁BrClN₃OS
Molecular Weight:408.706
Hs Code.:

Synonyms:1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

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Technology Process of 1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

There total 5 articles about 1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 117320-61-3
5-(3-chlorophenyl)-4H-1,2,4-triazole-3-thiol

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 117320-70-4
1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

Guidance literature:: With potassium hydroxide; In ethanol; Reflux;
DOI:10.1016/j.biopha.2017.07.139

Reference yield:

: 881-74-3
2-(3-chlorobenzoyl)hydrazinecarbothioamide

: 117320-70-4
1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / 8percent aq. NaOH / 3 h / Heating

2: methanol / 3 h / Heating

With sodium hydroxide; In methanol;

Reference yield:

: 1673-47-8
3-chlorobenzhydrazide

: 117320-70-4
1-(4-Bromo-phenyl)-2-[5-(3-chloro-phenyl)-4H-[1,2,4]triazol-3-ylsulfanyl]-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride

2: sodium hydroxide

3: potassium hydroxide / ethanol / Reflux

With hydrogenchloride; potassium hydroxide; sodium hydroxide; In ethanol;
DOI:10.1016/j.biopha.2017.07.139